Microscale Organic Laboratory: with Multistep and Multiscale Syntheses

Customer Reviews:

It is not that bad.......2003-12-15

This is my first semester organic chemistry course. Even though I have been using another book for laboratory "Organic Chemistry Lab [...] by Charles E., Jr. Bell", this book helped me to understand the concepts better (many times the instructor quized us on the reasoning behind an experiment which Bell does not mention).
Moreover, Bell's book is somewhat incomplete. For about 25% of the experiments that I performed, we used hand-outs because Bell's did not handle them correclty.
I think that "developing microscale techniques" section was really good to introduce you to the most important techniques that one must master (which Bell does not mention much either.) I think that this book is not as bad as the other reviewers think, at least, relatively not as bad as they might think.

A very bad book.......2003-09-10

This is one of the worst textbooks I have ever used. Luckily, we only used to for one week...I couldn't imagine having to use it for any longer than that. Unfortunately there isn't an option for zero stars.

The worst book I have EVER had........2003-06-04

I have had some terrible professors, but I have NEVER had a book that was as insufficient and wholly undeveloped in its topic. Mayo et al. may know what they are doing in the laboratory, but they must know NOTHING of writing books to convey knowledge. Someone told me that this is the most widely used book for organic chemistry labs. If that is true, I hate to see the sad state of science in a few years when we start to see all the chemists it produces. Because of the overwhelming difficulty of the problems in this book, students are forced to concentrate on specific answers to the questions that are asked and not on the concepts overall. The result: for all the complexity and effort involved, the student learns NOTHING. The second half of the book outright states (in the intro to Chapter 7) that "the mechanisms ... are more involved and not generally developed at the introductory level." I am an undergraduate student whose second semester of organic chemistry lab far outstrips the two- semester academic textbook.

This book is horrible.......2003-05-01

Chances are you are not buying this book for your home organic lab. You probably are buying this for a class. I feel sorry for you.

Don't buy this!.......1997-12-16

I used this text for my organic labs (2 semesters, for majors). I thought the book was pitiful. From the undergrad's perspective, it was disorganized, unclear, verbose; generally excessive. The black and white pages with black line figures are not exactly a pleasure to read. I HAD to buy it. I hope you don't!

Organic Chemistry Laboratory: Standard and Microscale Experiments

Average customer rating:

Strong Coverage of Spectroscopy, interesting labs

Organic Chemistry Laboratory: Standard and Microscale Experiments
Charles E. Bell , Douglas Taber , and K. Clark
Manufacturer: Brooks Cole
ProductGroup: Book
Binding: Hardcover

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The Organic Chem Lab Survival Manual, A Student's Guide to Techniques
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ASIN: 0030292727

Book Description

The new edition continues to offer a wide variety of organic lab experiments for both standard and microscale formats and features unusually strong coverage of spectroscopy.

Customer Reviews:

Strong Coverage of Spectroscopy, interesting labs.......2001-04-15

This book contains an exceptionally strong coverage of spectroscopy. Proton and carbon NMR are well explained, with detailed tables to predict and justify chemical shifts. IR spec is also well explained. A limited discussion of mass spec is also present. The laboratory exercises are clear in most cases, with a few minor exceptions. Be sure to read the instructions before lab as a few exercises contin ambiguous instructions that become more clear if the entire lab is read first. The number of syntheses is excellent, and many laboratory exercises contain interesting procedures that result in various colored, or common products. As a student of one of the authors, Dr. Douglas F. Taber, I have found this book to be a useful reference for spectroscopy as well as an excellent lab text.

Introduction to Organic Laboratory Techniques: Microscale Approach

Average customer rating:

Good content, poor construction
Book in great shape
AN ABSOLUTE TREASURE!
Excellent Lab Text But Not Everyone Has To Buy It
Best organic laboratory manual available!

Introduction to Organic Laboratory Techniques: Microscale Approach
Donald L. Pavia
Manufacturer: Brooks Cole
ProductGroup: Book
Binding: Hardcover

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ASIN: 0030265665

Book Description

This edition features the successful format that has characterized the previous editions. It includes essays that add relevance and interest to the experiments, and emphasis on the development of the important laboratory techniques, the use of spectroscopy and instrumental methods of analysis, a section featuring conventional-scale experiments and methods, and a wide selection of well-tested and well-written experiments.

Customer Reviews:

Good content, poor construction.......2006-11-10

Having owned the previous version of this book, I would have to say that the layout in this new version is much more linear and easy to follow. In addition to new experiments, the instructions are clear for a beginning organic lab student. That being said, however, the material that the book is constructed from is sub par...the pages are very delicate, seeming to be made of tissue paper...Over all, I would recommend this book for its content, but not for the craftsmanship.

Book in great shape.......2005-09-19

Book is flawless, not even scratches on the cover, cannot remember promptness of delivery.

AN ABSOLUTE TREASURE!.......2001-07-25

Pavia et al's Organic Laboratory Techniques (2nd Ed) is an astonishingly excellent book for the beginning student.

In great (yet delightful) detail it describes a series of 60 varied experiments designed to acquaint the reader with a plethora of laboratory techniques, from Measuring Volumes and Weights up thru Chromatography and Spectroscopy.

Particularly good are the many exceptionally clear drawings of laboratory apparatus, and rational behind the instrumentation. (Eg, do you know why you should put a trap in the aspirator hose, or for that matter how the aspirator (vacuum) works?) Sprinkled throughout are hints on how best to perform this, that or the other thing.

A thorough reading of this gem will make you right at home in the organic chemistry laboratory, and indeed will practically make you an organic chemist in spite of yourself.

In fact, if you are thinking of going to college, you might ask whether this text is used in the college's Organic Chemistry Lab course. If not, and you are interested in science, find a school that uses it! And if you are already in a lab course with another text, you would be well advised to get this eminently readable treasure also.

Excellent Lab Text But Not Everyone Has To Buy It.......2000-08-29

Though a complete laboratory text with 50+ experiments, lab techniques, tables of unknowns and spectroscopy, the organic faculty prepare our own lab manual to be followed. Pavia text becomes a close handy reference for lab techniques and setup. The techniques section, which include filtration, crystallization, distillation (simple, fractional, and steam), chromatogrpahy (column, thin-layer, and gas)... should be carefully studied before conducting experiments for beginning students. Unless your organic lab course follows almost exactly the outline of experiments in this text, you can check it out from the library and read it.

Best organic laboratory manual available!.......1999-05-17

I have taken a full course using this book and I think that it is the best one I have seen! Organic chemistry is a hard subject and this book lays it out in an understandable way. The "techniuques" section is current, readable, and the pictures are well done. The essays that accompany many of the experiments are entertaining and give good background information that helps doing the experiments more enjoyable. Probably the best section is the "identification of unknowns" section which lays out in a good logical way how to identify what you have in the lab. I think that the book also addresses and promotes a great trend in chemistry i.e. microscale research that reduces waste and promotes conservation of chemicals and the environment.

Macroscale and Microscale Organic Experiments

Average customer rating:

Very practical text to be used in the organic laboratory

Macroscale and Microscale Organic Experiments
Kenneth L. Williamson , Robert Minard , and Katherine M. Masters
Manufacturer: Houghton Mifflin Company
ProductGroup: Book
Binding: Hardcover

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ASIN: 0618590676

Book Description

This flexible, reliable, accurate manual includes both macroscale and microscale procedures for each experiment. The level and writing style of the text, which emphasizes biochemical and biomedical applications, make it ideally suited for the mainstream organic chemistry laboratory.

Microscale experiment options allow instructors to purchase costly chemicals in small quantities while minimizing issues of environmental impact and hazardous waste disposal. Macroscale versions can be used for less costly experiments, giving students experience with the manipulation of conventional glassware.

A student CD-ROM includes videos and photos related to the material in the text. Videos feature the exact glassware required for each experiment and demonstrate techniques for how to conduct experiments successfully and safely. Photos show lab equipment set-ups.
Icons throughout the text direct students to the corresponding videos and photos on the CD-ROM. A letter or number code allows students to search the CD-ROM for the appropriate technique.
"In this Experiment" is a new feature that appears before every microscale experiment. It presents the objective of the experiment and keeps students from getting bogged down in the minute details of experimental procedures.
An instructor web site provides a forum where instructors can communicate directly with the text author about specific experiments and the implementation of microscale techniques. The site also includes PDF files from the Instructor's Resource Manual.
Material on mass spectroscopy has been added to Chapter 14.

Customer Reviews:

Very practical text to be used in the organic laboratory.......1998-08-28

Simply excellent. It provided adequate theory behind each of the experiments while explaining the experiments' procedures step by step.

Microscale Heat Transfer - Fundamentals and Applications: Proceedings of the NATO Advanced Study Institute on Microscale Heat Transfer - Fundamentals and ... II. Mathematics, Physics and Chemnistry)

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Microscale Heat Transfer - Fundamentals and Applications: Proceedings of the NATO Advanced Study Institute on Microscale Heat Transfer - Fundamentals and ... II. Mathematics, Physics and Chemnistry)

Manufacturer: Springer
ProductGroup: Book
Binding: Paperback

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This volume provides a comprehensive state-of-the art assessment of the fundamentals of the Microscale heat transfer and transport phenomena and heat transfer and applications in Microsystems. The modern trend toward miniaturization of devices requires a better understanding of heat mass transfer phenomena in small dimensions. Devices having dimensions of order of microns are being developed for use of cooling of integrated circuits, and in biochemicals-biomedical applications and cryogenics. Microelectromechanical systems (MEMS) have an important impact in medicine, bioengineering, information technologies and other industries.

Techniques in Organic Chemistry: Miniscale, Standard-Taper Microscale, Williamson Microscale

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Techniques in Organic Chemistry: Miniscale, Standard-Taper Microscale, Williamson Microscale
Jerry R. Mohrig , Christina Noring Hammond , Paul F. Schatz , and Terence C. Morrill
Manufacturer: W. H. Freeman
ProductGroup: Book
Binding: Paperback

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Experimental Organic Chemistry: Standard and Microscale

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Experimental Organic Chemistry: Standard and Microscale
Laurence M. Harwood , Christopher Moody , and Jonathan M. Percy
Manufacturer: Blackwell Publishing Limited
ProductGroup: Book
Binding: Paperback

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Book Description

This established text continues to provide a rigorous account of the principles and practice of experimental organic chemistry, taking students from their first day in the laboratory right through to research work. New to this edition, a microscale approach has been integrated into the entire text, alongside conventional manipulations, bringing it in line with current laboratory practice. Maintaining the unique structure of the previous edition, the first half of the book surveys all aspects of safe laboratory practice, the use of a wide range of purification and analytical techniques, particularly spectroscopic analysis. The second half contains easy-to-follow experimental procedures, each designed to illustrate an important reaction type of basic principle of organic chemistry. Tried and tested over the past decade, these experiments are graded according to their complexity and many of these have microscale equivalents. Of prime importance, all aspects of health and safety in the laboratory have been updated according to the latest guidelines and are highlighted throughout the text.

Modern Projects and Experiments in Organic Chemistry: Miniscale and Williams on Microscale

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Modern Projects and Experiments in Organic Chemistry: Miniscale and Williams on Microscale
Jerry R. Mohrig , Christina Noring Hammond , Terence C. Morrill , and Paul F. Schatz
Manufacturer: W. H. Freeman
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Microscale and Miniscale Organic Chemistry Laboratory Experiments

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Microscale and Miniscale Organic Chemistry Laboratory Experiments
Allen M Schoffstall , Barbara A Gaddis , Melvin L Druelinger , Allen Schoffstall , Barbara Gaddis , and Melvin Druelinger
Manufacturer: McGraw-Hill Science/Engineering/Math
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Organic Chemistry Demystified

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Book Description

This book offers a comprehensive introductory treatment of the organic laboratory techniques for handling glassware and equipment, safety in the laboratory, micro- and miniscale experimental procedures, theory of reactions and techniques, relevant background information, applications and spectroscopy.

Average customer rating:

Macro / Microscale Organic Experiments
Kenneth L. Williamson
Manufacturer: Houghton Mifflin Company
ProductGroup: Book
Binding: Hardcover

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The market leader for the full-year organic laboratory, this manual derives many experiments and procedures from the classic Feiser lab text, giving it an unsurpassed reputation for solid, authoritative content. The Williamson/Minard/Masters manual's flexible mix of macroscale and microscale options for most experiments allows instructors to save on the purchase and disposal of expensive, sometimes hazardous organic chemicals. Macroscale versions can be used for less costly experiments, giving students experience working with conventionally sized glassware.

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