Book Description
Originally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book:
- Uses a problem-solving approach with extensive reference charts and tables.
- Offers an extensive set of real-data problems offers a challenge to the practicing chemist
Customer Reviews:
Excellent excercises..........2006-03-12
It's an OK book if you are a novice in the Spectroscopy determination area, but a very nice book if it's going to be used as a reference book. It's very handy and explains the principles of the Spectroscopic and Spectrometric determinations in a very understandable way. Moreover, the excercises are challenging, making this book and excellent tool for those students interested in learning how to determine structures out of some spectra, although the spectra sometimes are so clean that they don't correspond with the one's that are taken by routine. The weak points of this book are the IR chapter and the lack of a UV chapter explaining various useful techniques for structural determination such as ORD and CD. The NMR section is just OK, but there are more details to be explained in the 2-D NMR NOESY, TOCSY and ROESY. I think the Mass Chapters are the best that any single book has offered to me so far to understand quite easily how powerful is the GCMS as a tool for the Structural Determination of Organic Compounds.
Reference vs. Teaching Material.......2005-03-05
This book has wonderful charts and tables for quick referencing, however it is sorely lacking in demonstrations and worked out examples for students new to the subject. The chapters are painfully slow and complex when explaining the theory behind the spectrometric methods and effects on classes of molecules. In short, don't use this book to learn the material unless you already know it. It is a comprehensive reference, but not an effective textbook to teach from.
Great material, regular text..........2001-07-17
The book is subdivided into only 3 of the 4 classical methods for spectrometric identification of compounds: IR, MS, and finally NMR (covering 1H, 13C and very little of 19F and 31P). UV is left out in this edition, so maybe getting a hold of the old edition's UV chapter (which is extremely well-written) might be desired. The MS and the IR chapters are also well-written and explained out. It is in the main technique (NMR) that the author fails to deliver the subject in a straightforward manner and lacks what I think is most important in this field: a large number of exercises and problems.
An Important book.......2000-05-10
This book provide a the basis of the fundamentals of Spectroscopy in many fields (IR, HNMR, CNMR, DEPT, COSY, HMBC, HMQC, TOCSY, MS, and much more) It has many real problems in an special chapter. And the most important, it has a lot of important tables and spectrums.
Good in NMR Spectra analysis information, but weak elsewhere.......1999-11-19
This book lacked information in my opinion. Silverstein started a good project but just didn't give enough information about IR interpretation, mass spec, C-13 NMR, etc. He focussed on 2-D NMR a great deal, and I believe that there are much better textbooks on this subject.
Book Description
The Fourth Edition of Greene's Protective Groups in Organic Synthesis continues to be an indispensable reference for controlling the reactivity of the most common functional groups during a synthetic sequence. This new edition incorporates the significant developments in the field since publication of the third edition in 1998, including...
- New protective groups such as the fluorous family and the uniquely removable 2-methoxybenzenesulfonyl group for the protection of amines
- New techniques for the formation and cleavage of existing protective groups, with examples to illustrate each new technique
- Expanded coverage of the unexpected side reactions that occur with protective groups
- New chart covering the selective deprotection of silyl ethers
- 3,100 new references from the professional literature
The content is organized around the functional group to be protected, and ranges from the simplest to the most complex and highly specialized protective groups.
Customer Reviews:
glad i bought it.......2007-08-31
i'm do organic synthesis. i reference this one once a week on average. it's the first stop whenever a protecting group questions comes up.
A must have for any synthetic laboratory.......2006-04-27
There are other protecting group books out there but I found this one to be the most comprehensive and easy to use.
must have.......2006-02-24
if you are synthetic chemist you ought to have this book with you
Protecting my thesis.......2004-08-15
This book contains methods for the installation and removal of practically every protecting group you can think of, and likely some you've never encountered. Most methods are referenced to articles containing representative procedures, saving valuable time scouring the literature. It is compact, well-organized and reasonably priced. Along with March's Advanced Organic Chemistry, this book is a must have for any organic chemist.
The Book Will be Your Bible in Lab.......2002-02-04
If you doing any sort of organic chemistry in the lab, you will really get your hands into this handy reference on protecting groups. The book neatly organized into functional groups and their protecting groups. A Primer for organic chemists. It will save you zillion hours of researching for papers/references on the appropriate protecting groups used in reactions.
Average customer rating:
- Organic Spectroscopy Made Clear
|
Organic Structure Analysis (Topics in Organic Chemistry)
Phillip Crews ,
Jaime Rodriguez , and
Marcel Jaspars
Manufacturer: Oxford University Press, USA
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Binding: Hardcover
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Structure Determination of Organic Compounds: Tables of Spectral Data
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Principles of Polymerization
ASIN: 0195101022 |
Book Description
Organic Structure Analysis is an ideal text for upper-level undergraduate and first-year graduate courses in organic spectroscopy. It provides students with the background necessary to effectively apply spectroscopic data in establishing features of molecular structure. Unique in its coverage, it is the only text that emphasizes strategies, interpretation, modern techniques, and problem solving. The text's major aim is to show how spectra can be efficiently examined in order to identify a molecule's major structural elements. It focuses on four techniques which are used on a day-to-day basis by most organic chemists: nuclear magnetic resonance (NMR), mass spectroscopy (MS), infrared (IR), and ultraviolet-visible (UV-VIS). Each chapter provides different perspectives on using spectroscopic data in a step-by-step process to establish structural features such as an overall carbon framework; the presence and location of functional groups; the regiochemistry and stereochemistry of substituents; and, finally, the absolute stereochemistry of chiral centers. Recent advances in NMR and MS have changed the way these components are introduced and used in organic spectroscopy courses. Unlike similar texts, this book provides ample, up-to-date coverage of the latest developments in NMR and MS techniques. Organic Structure Analysis adopts a practical approach to the subject which emphasizes building experience; the authors recognize that a combination of problem solving, access to data from models, and understanding the rules of spectral interpretation helps students to build expertise in structure determination from spectra. It outlines elements of theory, but with an emphasis on those directly relevant to spectral interpretation. The text is divided into three major sections; the first section provides extensive coverage of each of the individual methods, the second section illustrates how the strategies of organic structure are actually applied in ten problems whose solutions are provided, and the third section consists of fifty unsolved problems which range from simple monofunctional compounds to complex natural products.
Customer Reviews:
Organic Spectroscopy Made Clear.......2001-08-24
Crews is not a hardcore treatise of the subject. It does not cover the quantum mechanics behind spectroscopy and the complicated mathematical underneath the concept. Instead it discusses the fundamentals and results of such quantum calculations which apply to identification of organic compounds. Basic concepts of nuclear magnetic resonance, infrared spectroscopy, ultra violet spectroscopy are thoroughly covered with examples and charts. Crews is a splendidly-written, straight-forward work that would be suitable for advanced undergraduates who had finished at least one year of organic chemistry, for those who pursue chemical research, and entering grad students.
Book Description
A true introductory text for learning the spectroscopic techniques of Nuclear Magnetic Resonance, Infrared, Ultraviolet and Mass Spectrometry. It can be used in a stand alone spectroscopy course or as a supplement to the sophomore-level organic chemistry course.
Customer Reviews:
A must-have for learning Spectroscopy!.......2007-08-17
I absolutely LOVE this book. I first bought it for my Junior year analytical chemistry class, and I still use it today in grad school. It is VERY good at explaining NMR theory. Anything I ever needed related to NMR or IR I found in this book. It is by far the most useful chemistry book I own.
Dated.......2003-04-11
Standard textbook outlining most spectroscopic techniques as taught at undergraduate level. However, contains an embarrassingly dated treatment of mass spectrometry which can not have been rewritten since the 1970s. No mention of the biggest MS techniques in use today (electrospray and MALDI), a glaring oversight especially in light of Fenn & Tanaka winning Nobel Prizes in 2002 for just these developments. And time-of-flight instruments having a mass range of 5000 and resolution of 200? Several years before this book was published, commercial machines were available with mass ranges well over 100,000 Da and resolutions of 10,000+. Not only poor, but misleading. Overall, a rather derivative book that seems to have been written largely by consultation of more authoritative work (probably an early edition of Williams & Fleming).
Another Good Reference on Organic Spectroscopy.......2001-08-24
The new edition of Pavis might be the twin to Crews' Organic Structural Analysis. This text discusses the fundamentals of 1H NMR, carbon-13 NMR, infrared spectroscopy, UV spectroscopy. The book also includes a section on 2D NMR. Pavia should not be missed by advanced undergraduate students who pursue research and practicing chemists who need quick reference on interpreting spectra.
An Essential Introductory Reference.......2001-05-22
This book is probably the best introductory reference on spectroscopy currently available, and I've checked out pretty much every book on the market right now. I'm a chemist, and this book got me through my senior synthesis and spectroscopy lab. Proton and carbon-13 NMR, IR, GC/MS, and UV/Vis are all covered in the book. It includes many handy tables of characteristic shifts for NMR, characteristic absorbances for IR and UV/Vis, and a nifty table on common GC/MS fragments by m/e. The chapter on 2D NMR is lousy, but that's not really introductory material anyhow. The UV/Vis chapter is kind of cursory, but UV/Vis isn't all that useful.
This is a book that I intend to hang on to for a while.
Great books for students in chemistry.......1999-06-05
I have found this book to a great tool for students of organic chemistry especially those wanting to further their education in graduate school or medical school.It is eay to read and can also be used a "teach yourself" book. I recomend this book to anyone who is a bit shaky in interpreting NMR, IR, and Mass Spec.
Average customer rating:
|
Synthesis and Applications of Isotopically Labelled Compounds, Volume 7
Manufacturer: John Wiley & Sons
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Binding: Hardcover
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ASIN: 0471495018 |
Book Description
This outstanding book covers the most recent advances in the production of stable and radioactive isotopes as well as in the synthesis, analysis and applications of isotopically labelled compounds. Written by internationally renowned contributors, it provides authoritative and wide-ranging coverage of significant growth areas including:
- new methodologies in the production of isotopes
- novel approaches to compounds labelled with isotopes of hydrogen, carbon and other stable, long-lived and short-lived radioactive isotopes
- advances in the analysis of istopically labelled compounds
- recent and future applications of isotopes in pharmaceutical research and development, in pharmacological and clinical sutdies and nuclear medicine, as well as in agricultural, nutritional and environmental research
- recent applications of isotopes in investigating organic and bioorganic mechanisms and pathways
- safety and regulations of handling isotopes
This will be an invaluable information and reference source to anyone involved in the production of isotopes, the synthesis and analysis of compounds labelled with stable, long-lived or short-lived radioactive isotopes, in drug research and development, in clinical investigations and nuclear medicine, in agricultural research and development and environmental investigations, in the elucidation of biological and chemical pathways, handling radioisotopes, laboratory design and other areas.
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Phosphoric Anhydride: Structure Chemistry and Applications
D. A. Efremov ,
J. C. Tebby , and
P. A. Zavlin
Manufacturer: John Wiley & Sons
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ASIN: 0471985082 |
Book Description
Phosphoric Anhydride is a unique reagent in organic synthesis which is involved in reactions of dehydration, dealcoholysis, phosphorylation, condensation, rearrangement and catalysis, amongst others. Producing numerous organic and inorganic phosphates which are used in the textile, food and drink, and paper and plastics industries, phosphoric anhydride is a valuable and versatile starting material. Phosphoric anhydride and its derivatives are of particular importance in biochemistry as a phosphorylating agent. Phosphoric Anhydride addresses researchers, industrial chemists and advanced students in organic, organophosphorus, biological, inorganic and chemical technology. Contents Introduction Preparation Structure and physico-chemical properties Reactivity Phosphoric anhydride in the evolution of life Phosphoric anhydride and its derivatives in biological chemistry Applications References Index
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|
Wood and Cellulosic Chemistry, Second Edition Revised and Expanded
David N.-S. Hon , and
Nobuo Shiraishi
Manufacturer: CRC
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ASIN: 0824700244 |
Book Description
Revised and expanded for the second edition, this text details the principal concepts and developments in wood science, chemistry and technology. It includes new chapters on the chemical synthesis of cellulose and its technology, preservation of wood resources and the conservation of waterlogged wood.
Book Description
This book has so closely matched the requirements of its readership over the years that it has become the first choice for chemists all over the world.The fourth edition retains its original aims to teach the fundamentals of heterocyclic reactivity and synthesis in a way that is understandable to second- and third-year undergraduate chemistry students. It is important to emphasise that the more advanced sections of the book make it an important reference work for chemists at all levels who are working with heterocyclic compounds in industry.New sections deal with heterocyclic aspects of combinatorial chemistry, bioprocessing, and conducting polymers.
Customer Reviews:
Valuable reference to all facets of heterocyclic chemistry.......1999-08-28
This book gives a thorough review of the chemistry of each particular class of heterocycles, covering structure, reactivity, and synthesis. Unique to this book is a coverage of the organometalic chemistry associated with each class. It is my opinion that this book is a touch better than the Thieme and Gilcrest heterocyclic books, based mostly on the organization of material. I do wish, however, that the authors had given aminoheterocycles a bit more attention!
Average customer rating:
- It is a good book but difficult to read.
- A concise and beautifully written book on stereochemistry.
|
Stereochemistry of Coordination Compounds (Inorganic Chemistry: A Textbook Series)
Alexander von Zelewsky
Manufacturer: John Wiley & Sons
ProductGroup: Book
Binding: Paperback
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ASIN: 0471950572 |
Book Description
This well-illustrated and well-referenced book provides a systematic introduction to the modern aspects of the topographical stereochemistry of coordination compounds, which are made up of metal ions surrounded by other non-metal atoms, ions and molecules.
Customer Reviews:
It is a good book but difficult to read........1999-04-18
Zelewsky's book covers an important topic which is typically not covered in detail in graduate classes in inorganic chemistry. Although the book is somewhat difficult to read, which is probably because the author is not a native English speaker, it is worth wading through.
A concise and beautifully written book on stereochemistry........1997-11-19
The book explains the modern aspects of stereochemistry of coordination compounds including nomenclature, chirality elements, isomer counting, helices, chains and knots, gives an account of the historical background and includes many 3D-figures as stereograms. All figures and additional material are available on the internet. The book is well suited for undergraduates, post-graduates and especially lecturers who can benefit from the supplementary material available. Just colors are missing - but this for the sake of a really affordable price.
Average customer rating:
- Good but complicated
- Chemistry book review
- Excellent reference book
- Great book for environmental chemistry
- Outstanding text and reference
|
Environmental Organic Chemistry (Environmental Science and Technology Series)
Rene P. Schwarzenbach ,
Philip M. Gschwend , and
Dieter M. Imboden
Manufacturer: Wiley-Interscience
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Environmental Organic Chemistry: Illustrative Examples, Problems, and Case Studies
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ASIN: 0471839418 |
Book Description
Environmental Organic Chemistry focuses on environmental factors that govern the processes that determine the fate of organic chemicals in natural and engineered systems. The information discovered is then applied to quantitatively assessing the environmental behaviour of organic chemicals. Now in its 2nd edition this book takes a more holistic view on physical-chemical properties of organic compounds. It includes new topics that address aspects of gas/solid partitioning, bioaccumulation, and transformations in the atmosphere.
- Structures chapters into basic and sophisticated sections
- Contains illustrative examples, problems and case studies
- Examines the fundamental aspects of organic, physical and inorganic chemistry - applied to environmentally relevant problems
- Addresses problems and case studies in one volume
Download Description
A troubling answer to the most critical question facing today's world energy market-can Saudi Arabia meet the rising world demand for oil in the years ahead Sparked by personal observations of Saudi oil wells-which led him to suspect that some Saudi fields were in decline-energy industry insider Matt Simmons has created a compelling case that Saudi Arabia's production will soon reach an apex, after which the world will be confronted with an immense and potentially catastrophic oil shortage. Written in a clear and engaging style, Twilight in the Desert provides an in-depth look at the world oil market and the mismanagement of Saudi oil resources. This factually based book is backed by over 200 technical papers-all published over the last 20 years-that individually detail problems with particular Saudi oil wells and fields, and collectively demonstrate how the entire Saudi system could stall under the pressure of higher world oil demand. Based on his analysis, Mr. Simmons asserts that sudden and sharp oil production declines could happen at any time. Twilight in the Desert shows that even under the most optimistic scenario, Saudi Arabia may be able to maintain current rates of production for several years, but will not be able to increase production enough to meet the expected increase in global demand. Eventually, the reckoning day will come, and the world economy will be confronted with a major shock that will stunt economic growth, increase inflation, and further destabilize the Middle East. Matthew R. Simmons (Houston, TX) is Chairman and Chief Executive Officer of Simmons & Company International, a Houston-based investment bank that specializes in the energy industry. He currently serves on the boards of The Atlantic Council of the United States and Brown Forman Corporation, and is a member of the National Petroleum Council and the Council on Foreign Relations.
Customer Reviews:
Good but complicated.......2007-03-09
I am using this book as part of my graduate class. Before I got this book, I was using the old edition, believe me the old edition is much simpler, easier to understand than this new one. They have integrated the book with overwhelming symbols for which they do not even have the key/index. You spend a lot of time figuring out what the symbols mean. So, I would recommend that you try to get a hold of the old edition of the book, however remember that the old edition does not cover the modelling part and does not give you exposure to the problem sets.
So, the bottom line is that if you want to get an understanding and feel of the subject goahead for the old edition, but if this is your core area of research and do not mind a bit of complication in the writing and explanation, go for the new edition.
Chemistry book review.......2006-02-25
This is a very good book to use to learn about the fate and transport of organic material through the environment.
Excellent reference book.......2003-08-15
This book is an asset for the student and professional alike.
Great book for environmental chemistry.......2001-12-28
I have used this book while taking a course in environmental chemistry. This book is easy to read, understand and really simplified a very complex and interesting topic. It covers wide range of topics in envrionmental chemistry. I really recommend my fellow students to get this book !
Outstanding text and reference.......1999-12-31
A must have for students and researchers in the field of environmental chemistry. This text pulls together fundamental concepts regarding fate and transport of organic pollutants in a comprehensive and logical manner. I enjoyed reading it the first time when I was using it as a course text, and it has been invaluable as a reference during my research.
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