Introduction to Organic Laboratory Techniques: Microscale Approach
Average customer rating: 4.5 out of 5 stars
  • Good content, poor construction
  • Book in great shape
  • AN ABSOLUTE TREASURE!
  • Excellent Lab Text But Not Everyone Has To Buy It
  • Best organic laboratory manual available!
Introduction to Organic Laboratory Techniques: Microscale Approach
Donald L. Pavia
Manufacturer: Brooks Cole
ProductGroup: Book
Binding: Hardcover

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ASIN: 0030265665

Book Description

This edition features the successful format that has characterized the previous editions. It includes essays that add relevance and interest to the experiments, and emphasis on the development of the important laboratory techniques, the use of spectroscopy and instrumental methods of analysis, a section featuring conventional-scale experiments and methods, and a wide selection of well-tested and well-written experiments.

Customer Reviews:

4 out of 5 stars Good content, poor construction.......2006-11-10

Having owned the previous version of this book, I would have to say that the layout in this new version is much more linear and easy to follow. In addition to new experiments, the instructions are clear for a beginning organic lab student. That being said, however, the material that the book is constructed from is sub par...the pages are very delicate, seeming to be made of tissue paper...Over all, I would recommend this book for its content, but not for the craftsmanship.

5 out of 5 stars Book in great shape.......2005-09-19

Book is flawless, not even scratches on the cover, cannot remember promptness of delivery.

5 out of 5 stars AN ABSOLUTE TREASURE!.......2001-07-25

Pavia et al's Organic Laboratory Techniques (2nd Ed) is an astonishingly excellent book for the beginning student.

In great (yet delightful) detail it describes a series of 60 varied experiments designed to acquaint the reader with a plethora of laboratory techniques, from Measuring Volumes and Weights up thru Chromatography and Spectroscopy.

Particularly good are the many exceptionally clear drawings of laboratory apparatus, and rational behind the instrumentation. (Eg, do you know why you should put a trap in the aspirator hose, or for that matter how the aspirator (vacuum) works?) Sprinkled throughout are hints on how best to perform this, that or the other thing.

A thorough reading of this gem will make you right at home in the organic chemistry laboratory, and indeed will practically make you an organic chemist in spite of yourself.

In fact, if you are thinking of going to college, you might ask whether this text is used in the college's Organic Chemistry Lab course. If not, and you are interested in science, find a school that uses it! And if you are already in a lab course with another text, you would be well advised to get this eminently readable treasure also.

4 out of 5 stars Excellent Lab Text But Not Everyone Has To Buy It.......2000-08-29

Though a complete laboratory text with 50+ experiments, lab techniques, tables of unknowns and spectroscopy, the organic faculty prepare our own lab manual to be followed. Pavia text becomes a close handy reference for lab techniques and setup. The techniques section, which include filtration, crystallization, distillation (simple, fractional, and steam), chromatogrpahy (column, thin-layer, and gas)... should be carefully studied before conducting experiments for beginning students. Unless your organic lab course follows almost exactly the outline of experiments in this text, you can check it out from the library and read it.

5 out of 5 stars Best organic laboratory manual available!.......1999-05-17

I have taken a full course using this book and I think that it is the best one I have seen! Organic chemistry is a hard subject and this book lays it out in an understandable way. The "techniuques" section is current, readable, and the pictures are well done. The essays that accompany many of the experiments are entertaining and give good background information that helps doing the experiments more enjoyable. Probably the best section is the "identification of unknowns" section which lays out in a good logical way how to identify what you have in the lab. I think that the book also addresses and promotes a great trend in chemistry i.e. microscale research that reduces waste and promotes conservation of chemicals and the environment.
Introduction to Organic Laboratory Techniques: A Small-Scale Approach (Brooks/Cole Laboratory Series for Organic Chemistry)
Average customer rating: 3.5 out of 5 stars
  • Introduction to Organic Laboratory Techniques : A Small-Scale Approach (Brooks/Cole Laboratory Series for Organic Chemistry)
  • WWU grad
  • Don't sell this book back!
Introduction to Organic Laboratory Techniques: A Small-Scale Approach (Brooks/Cole Laboratory Series for Organic Chemistry)
Donald L. Pavia , Gary M. Lampman , George S. Kriz , and Randall G. Engel
Manufacturer: Brooks Cole
ProductGroup: Book
Binding: Hardcover

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ASIN: 0534408338

Book Description

In this laboratory textbook for students of organic chemistry, experiments are designed to utilize standard-scale ("macroscale") glassware and equipment but with smaller amounts of chemicals and reagents. The textbook features a large number of traditional organic reactions and syntheses, as well as the isolation of natural products and experiments with a biological or health science focus. The organization of the text is based on essays and topics of current interest. There are six introductory technique-based experiments and eleven project-based experiments. In addition, there is a section of green chemistry experiments. The book contains a comprehensive treatment of laboratory techniques, including small-scale and some microscale methods.

Customer Reviews:

1 out of 5 stars Introduction to Organic Laboratory Techniques : A Small-Scale Approach (Brooks/Cole Laboratory Series for Organic Chemistry).......2005-09-14

It has taken this company a month to even send this book. It is quite amazing how slow this company and how it treats its customers. Do not expect books to come unless you want to wait til the book become a classic. Highly suggest to purchase from someone else. Luckly, I've been using a book from lab TA for my organic lab
class.

5 out of 5 stars WWU grad.......2003-09-05

Dr. Pavia's class was so much fun. It was great to have a book written for our facility, by our instructors. I recommend this book to other schools because the techniques are clearly explained and the experiments are interesting.

4 out of 5 stars Don't sell this book back!.......2002-09-20

An outstanding lab text for sophomore level 1-yr organic courses. Any chemistry/physical science major should not sell this book back at the end of the semester! Half of the book is dedicated to experiments which while informative is not the real gem here. The other half of the book covers techniques in organic and microscale chemistry. If you ever need to build a chromatographic column or do vacuum filtration again, you will be glad that you kept this book in your library.

The techniques section alone justifies buying this book. Chemistry majors, microbiologists, environmental scientists and engineers will all find this text valuable in their future careers.
Introduction to Chemical Principles: A Laboratory Approach (Brooks/Cole Laboratory Series for Introductory Chemistry)
Average customer rating: Not rated
    Introduction to Chemical Principles: A Laboratory Approach (Brooks/Cole Laboratory Series for Introductory Chemistry)
    Susan A. Weiner
    Manufacturer: Brooks Cole
    ProductGroup: Book
    Binding: Paperback

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    ASIN: 0534407773

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    Don't go to the lab without it! INTRODUCTORY TO CHEMICAL PRINCIPLES: A LABORATORY APPROACH teaches you to collect and analyze experimental data with ease using 34 class-tested experiments. Work Pages and Report Sheets for each experiment offer a convenient and efficient way for you to record your data as you work. Advanced Study Assignments, Sample Calculations, and laboratory and safety procedures are just a few of the tools that will help you complete your lab experiments successfully.
    Computational Chemistry: Introduction to the Theory and Applications of Molecular and Quantum Mechanics
    Average customer rating: 4 out of 5 stars
    • Very good first intro to computational chemistry
    • Rough reading
    Computational Chemistry: Introduction to the Theory and Applications of Molecular and Quantum Mechanics
    Errol G. Lewars
    Manufacturer: Springer
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    ASIN: 1402074220

    Book Description

    Computational chemistry has become extremely important in the last decade, being widely used in academic and industrial research. Yet there have been few books designed to teach the subject to nonspecialists.
    Computational Chemistry: Introduction to the Theory and Applications of Molecular and Quantum Mechanics is an invaluable tool for teaching and researchers alike. The book provides an overview of the field, explains the basic underlying theory at a meaningful level that is not beyond beginners, and it gives numerous comparisons of different methods with one another and with experiment.
    The following concepts are illustrated and their possibilities and limitations are given:

    - potential energy surfaces;
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    - ab initio, AM1 and related semiempirical methods;
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    Topics are placed in a historical context, adding interest to them and removing much of their apparently arbitrary aspect. The large number of references, to all significant topics mentioned, should make this book useful not only to undergraduates but also to graduate students and academic and industrial researchers.

    Customer Reviews:

    5 out of 5 stars Very good first intro to computational chemistry.......2004-08-28

    The only other book I can compare this to is Cramer's, and this one is better suited to a first introduction into computatioal chemistry. I have taken one graduate quantum chemistry course, and this was more than enough background for understanding this book. This is the only text I know of (I asked my comp chem prof if he knew of any others) that walks through a Hartree Fock calculation step by step using an example. There are some mistakes in the formulas, but they are quite minor. All in all, I would recommend this book to anybody interested in beginning to learn about computational chemistry.

    3 out of 5 stars Rough reading.......2004-05-12

    Maybe there just isn't any way into the basics of modern computational chemistry.

    Lewars introduces the easy parts in a clear enough way. Potential energy surfaces make sense. Molecular mechanics has a good, intuitive feel - it's the springs-and-balls model, elaborated to include plane and dihedral angles, representing force fields derived from other sources.

    After that (i.e., after p. 80), it's quantum mechanics for a few hundred pages. The premise is that the layout of electrons across a molecule determines its chemistry, and that the wave function tells where the electrons will be. Since the wave equations can't be solved exactly for anything with two or more electrons (!), it's actually approximations to quantum. That leads to two levels of opacity: quantum itself, and all the facts that were scraped off in the approximation process. At this point, the chice is binary: become fluent in quantum, or move on. There are a few nuggets to be had for the non-fluent, including some of the techniques for solving these horrendous integrals. Mostly, though, I moved on.

    After the "ab initio" quantum mechanical methods, Lewars presents the semi-empirical models. These deal with simplified models of wave functions. Unlike ab initio methods, which stand on almost purely theoretical models, semi-empirical methods are informed by experimental data. They are based on the electron wave functions, as are the ab initio methods, but use approximations calibrated by experimental results. The book's final section presents density functional theory (DFT), another technique for estimating where the electrons will be.

    This book demands a lot of the reader, more than I came in with or had time to develop. I was able to use it to get a working vocabulary of the major kinds of computations, the general categories of approach to modeling, and a rough idea of the techniques and complexities involved. I need a little more information than that, but not the immediate leap into the deep end presented here.

    I look forward to a review by someone more knowledgeable. For now, my only real criticism of this book is lack of glossary. Initialisms and acronyms abound. It would have made the going a lot easier if the book had one place where I could refresh my memory on the dozens or hundreds of abbreviations.
    Introduction to Wine Laboratory Practices and Procedures
    Average customer rating: Not rated
      Introduction to Wine Laboratory Practices and Procedures
      Jean L. Jacobson
      Manufacturer: Springer
      ProductGroup: Book
      Binding: Hardcover

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      Book Description

      With the rapid growth of the wine industry, it has become increasingly important for not only the enologist and wine maker, but also cellar and laboratory staff to perform the routine wine making duties. Written by a practitioner with hands-on experience in the field, Introduction to Wine Laboratory Practices and Procedures provides a step-by-step guide on performing these essential tasks.

      Gently easing the reader into the more advanced concepts and analysis, the book covers vineyard sampling to bottling with sections on chemistry, safety, quality control, and general wine education.

      It's a must have for entry level wine chemists and enologists; students in junior college programs; small and large wineries; professional and home wine makers; winery production staff; or anyone wanting to learn about winemaking in an easy to understand format.

      Computational Methods in Physics, Chemistry and Biology: An Introduction
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        Computational Methods in Physics, Chemistry and Biology: An Introduction
        Paul Harrison
        Manufacturer: Wiley
        ProductGroup: Book
        Binding: Paperback

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        Introduction to Conventional Transmission Electron Microscopy (Cambridge Solid State Science)
        Average customer rating: 4.5 out of 5 stars
        • Wonderful Introduction to Transmission Electron Microscopy
        • Excellent
        Introduction to Conventional Transmission Electron Microscopy (Cambridge Solid State Science)
        Marc De Graef
        Manufacturer: Cambridge University Press
        ProductGroup: Book
        Binding: Paperback

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        ASIN: 0521629950

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        Download Description

        This book covers the fundamentals of conventional transmission electron microscopy (CTEM) as applied to crystalline solids. Emphasis is on the experimental and computational methods used to quantify and analyze CTEM observations. A supplementary website containing interactive modules and free Fortran source code accompanies the text. The book starts with the basics of crystallography and quantum mechanics providing a sound mathematical footing for the rest of the text. The next section deals with the microscope itself, describing the various components in terms of the underlying theory. The second half of the book focuses on the dynamical theory of electron scattering in solids including its applications to perfect and defective crystals, electron diffraction and phase contrast techniques. Based on a lecture course given by the author in the Department of Materials Science and Engineering at Carnegie Mellon University, the book is ideal for graduate students as well as researchers new to the field.

        Customer Reviews:

        4 out of 5 stars Wonderful Introduction to Transmission Electron Microscopy.......2007-02-16

        For my taste, this book is the best introduction to Transmission Electron Microscopy that I have read. It is written at a higher level than Williams and Carter. This book is probably best suited to students with a B.S. in Physics. At the very least one should have benefited from a two semester undergraduate course on Modern Physics (including such things as solving the Schrodinger Equation for the Hydrogen atom) before tackling this book. I wish that a book like this had been out thirty years ago when I started learning TEM! This book does a very good job on two-beam theory and has truly wonderful dispersion surface diagrams.

        5 out of 5 stars Excellent.......2003-08-21

        I took Prof. de Graef's class at CMU in 2001, and we used pre-prints of this text. Even in that mostly-finished form, it was excellent. It's only improved now that I have the finished, published form.

        Although I found the mathematical formalism that makes up the middle of this book excessive, it is important for people who will be modelling TEM experiments. The remainder of the book, on TEM basics, operation, and image/SADP interpretation, are all excellent.

        This book is an excellent CTEM text.
        Chemistry: An Introduction to General, Organic and Biological Chemistry Laboratory Manual (7th Edition)
        Average customer rating: Not rated
          Chemistry: An Introduction to General, Organic and Biological Chemistry Laboratory Manual (7th Edition)
          Karen C. Timberlake
          Manufacturer: Addison-Wesley
          ProductGroup: Book
          Binding: Paperback

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          Chemistry: An Introduction to General, Organic, and Biological Chemistry, Eighth Edition (Essential Laboratory Manual)
          Average customer rating: 5 out of 5 stars
          • Great job!
          Chemistry: An Introduction to General, Organic, and Biological Chemistry, Eighth Edition (Essential Laboratory Manual)
          Karen C. Timberlake
          Manufacturer: Benjamin Cummings
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          ASIN: 0805330062

          Book Description

          Drawing from the successful Laboratory Manual to accompany Chemistry: An Introduction to General, Organic, and Biological Chemistry, this lab manual includes 25 experiments that have been revised and updated. For college instructors and students, or anyone interested in general, organic, or biological chemistry.

          Customer Reviews:

          5 out of 5 stars Great job!.......2005-09-12

          This book was delivered before the due date and I was very satisfied with my order.
          Acceleration and Automation of Solid Sample Treatment (Techniques and Instrumentation in Analytical Chemistry)
          Average customer rating: Not rated
            Acceleration and Automation of Solid Sample Treatment (Techniques and Instrumentation in Analytical Chemistry)
            M.D. Luque de Castro , and J.L. Luque García
            Manufacturer: Elsevier Science
            ProductGroup: Book
            Binding: Hardcover

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            ASIN: 0444507167

            Book Description

            This book aims to provide scientists with information about a series of techniques that can be used with a view to facilitating the transformation of the sample to an appropriate state for subsequent detection or quantitation of its components of interest. The techniques dealt with range from the very simple ones (e.g. freeze-drying) to other more complex ones (e.g. glow discharge and laser-induced breakdown sampling).



            This is the first compilation ever on the subjects of acceleration of solid sample pretreatment; automation of solid sample pretreatment; and integration of solid sample pretreatment and detection. Readers will find here the information required to compare and select the best choice for each sample treatment need and ways to facilitate or automate the most complex and time-consuming step of the analytical process when solid samples are involved.

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            9. Modern Plastics Handbook
            10. Modern Quantum Chemistry: Introduction to Advanced Electronic Structure Theory

            Books Index

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