Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods

Book Description

This book offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. This book focuses on all aspects of NMR including classic methods, modern techniques, practical advice for execution of the NMR experiment, theory, and more. For practicing NMR spectroscopists who want a better understanding of their subject, professors who want a wider knowledge of NMR, preparative (synthetic) organic chemists in industry who want to have more information about how to prove the structures of the compounds they make, and analytical chemists in industry who actually carry out the experiments and want a better understanding of what they are doing.

Customer Reviews:

Excellent NMR book for the ones 'in between'.......2005-08-12

Lambert and Mazzola's NMR book strikes a nice balance between the weighty tomes aimed at NMR specialists, and the structure-determination only books aimed purely at synthetic organic chemists. For someone like me, who is interested in the experimental and technical aspects of the NMR spectrometer and of NMR spectroscopy, but only because he wants to run good, clean NMR experiments, this book is marvelous. Lambert combines concise and clear discussions of key concepts like relaxation, NOEs, phase cycling, and processing parameters, with succint and illustrative examples. One of the unique aspects of this book is the listing of ballpark parameters for many experiments including ones like mixing times, no. of scans, relaxation times etc. For all parameters, the essential things, and those essential things which you have to watch out for, are both carefully explained.
Lambert's book is a very useful tool for those chemists who are 'in between'- that is, those who want to do structure determination themselves and also learn the practical and fine points of spectral acquisition as well as processing, without too much detail, either instrumental or mathematical. Lambert and Mazzola give us just the right amount. A must have on the shelf of any scientist interested in NMR.

Experimental Organic Chemistry: Standard and Microscale

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Experimental Organic Chemistry: Standard and Microscale
Laurence M. Harwood , Christopher Moody , and Jonathan M. Percy
Manufacturer: Blackwell Publishing Limited
ProductGroup: Book
Binding: Paperback

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Organic Chemistry: Study Guide/Solutions manual
Elementary Principles of Chemical Processes
Differential Equations and Boundary Value Problems: Computing and Modeling, Third Edition
Molecular Biology of the Gene, Fifth Edition
Quantitative Chemical Analysis

ASIN: 0632048190

Book Description

This established text continues to provide a rigorous account of the principles and practice of experimental organic chemistry, taking students from their first day in the laboratory right through to research work. New to this edition, a microscale approach has been integrated into the entire text, alongside conventional manipulations, bringing it in line with current laboratory practice. Maintaining the unique structure of the previous edition, the first half of the book surveys all aspects of safe laboratory practice, the use of a wide range of purification and analytical techniques, particularly spectroscopic analysis. The second half contains easy-to-follow experimental procedures, each designed to illustrate an important reaction type of basic principle of organic chemistry. Tried and tested over the past decade, these experiments are graded according to their complexity and many of these have microscale equivalents. Of prime importance, all aspects of health and safety in the laboratory have been updated according to the latest guidelines and are highlighted throughout the text.

Experimental Organic Chemistry: A Small Scale Approach (2nd Edition)

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wish i was assigned a different text book
Everything a chemistry textbook should not be

Experimental Organic Chemistry: A Small Scale Approach (2nd Edition)
Charles F. Wilcox , and Mary F. Wilcox
Manufacturer: Prentice Hall
ProductGroup: Book
Binding: Hardcover

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Organic Chemistry (6th Edition) (Organic Chemistry) (Organic Chemistry)
Introduction to Spectroscopy (Saunders Golden Sunburst Series)
Solutions Manual to accompany Organic Chemistry
The Organic Chem Lab Survival Manual, A Student's Guide to Techniques
Organic Chemistry and CW+ GradeTracker Access Card Package (6th Edition)

ASIN: 002427691X

Book Description

Takes a small scale approach to experimentation, keeping costs of material and their disposal down by a factor of five coompared to standard scale, while retaining most standard scale equipment and requiring no special glassware. The previous edition ISBN is: 0-02-427620-0.

Customer Reviews:

wish i was assigned a different text book.......2006-03-11

was required by my school, thats why i cought it. has a lot of typos in it, and doesn't explain the experiemnts very well.
Very marginal over all

Everything a chemistry textbook should not be.......2005-05-22

Horribly written. Painfully disorganized, bouncing from technique to technique and concept to concept at COMPLETE random. Zero photo plates and minimal line drawings that aren't recognizable as anything actually seen in a laboratory. Structural formulas that look like they were produced in MS Word. In fact, the whole ugly layout has this appearance. The $107 price tag must have been a belabored attempt at humor.

Matrix-Isolation Techniques: A Practical Approach (Practical Approach Series)

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Matrix-Isolation Techniques: A Practical Approach (Practical Approach Series)
Ian R. Dunkin
Manufacturer: Oxford University Press, USA
ProductGroup: Book
Binding: Hardcover

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Book Description

Matrix isolation is a technique for trapping reactive species at very low temperatures and studying them spectroscopically. This book offers detailed practical advice on how to carry out matrix-isolation experiments, and is a unique introduction to the subject. Chapter 1 introduces a brief historical survey of the development of the technique that incorporates a discussion of its strength and limitations. Chapter 2 provides a thorough description of the building of a matrix-isolation laboratory from scratch. All the necessary equipment is described in full and there are diagrammatic examples throughout. In later chapters, ancillary equipment for generating reactive species, and an informative description of the various methods for forming low-temperature matrices are dealt with. There then follows a chapter on the specialized technique of matrix photochemistry with polarized light. The final chapter comprises an extensive collection of classic matrix experiments which have been selected due to their ease of application and which will thus serve as useful exercises for testing new pieces of equipment. This accessible text offers thorough coverage of the topic and will be invaluable to postgraduate and industrial chemists as an introduction to matrix isolation techniques. Researchers in chemistry and related fields who are considering whether matrix isolation can play a part in their own research will also find this book useful.

Average customer rating:

A phenomenal text by a phenomenal teacher
Student of the Publisher: Winter quarter 2004

Experimental Organic Chemistry
Daniel R. Palleros
Manufacturer: Wiley
ProductGroup: Book
Binding: Hardcover

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Organic Chemistry (with InfoTrac Printed Access Card)
Study Guide with Solutions Manual for McMurry's Organic Chemistry, 7th
Organic Chemistry (5th Edition)
Organic Chemistry
Prentice Hall Molecular Model Set For Organic Chemistry

ASIN: 0471282502

Book Description

This cutting-edge lab manual takes a multiscale approach, presenting both micro, semi-micro, and macroscale techniques. The manual is easy to navigate with all relevant techniques found as they are needed. Cutting-edge subjects such as HPLC, bioorganic chemistry, multistep synthesis, and more are presented in a clear and engaging fashion.

Customer Reviews:

A phenomenal text by a phenomenal teacher.......2005-10-14

Dr. Daniel Palleros is one of the finest experimental organic chemistry instructors in the University of California system, which is a truly impressive accomplishment. Dr. Palleros has for years been publishing and refining his experimental organic chemistry textbooks in-house at UC Santa Cruz, and has finally conglomerated the majority of his publications into a single, large, widely availible volume.

Dr. Palleros' writing style is engaging and accessible, covering both theory and application. His experiments are chosen excellently for diversity, challenge and depth. This volume is more than worth the price of admission, and would be an exceptional resource for any experimental organic chemistry insructor or student.

As a practicing (analytical) chemist, long since graduated, I still covet my now tattered advanced experimental organic chemistry 112L/M/N manuals and refer to them far more than any other college text in the subject, bar none. This volume has the advantage of being hardbound and professionally bound, and now serves as a much more durable replacement.

This volume has my Highest Possible recommendation.

Student of the Publisher: Winter quarter 2004.......2004-03-14

I think the book was excellent! And I would underline that word if I could. I am taking Daniel Palleros's Organic Chemistry right now. The only thing greater than his book is his teaching. I recommend it to any student or instructor teaching organic chemistry.

Experimental Organic Chemistry: A Miniscale and Microscale Approach (Brooks/Cole Laboratory Series for Organic Chemistry)

Average customer rating:

A great help

Experimental Organic Chemistry: A Miniscale and Microscale Approach (Brooks/Cole Laboratory Series for Organic Chemistry)
John C. Gilbert , and Stephen F. Martin
Manufacturer: Brooks Cole
ProductGroup: Book
Binding: Hardcover

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Organic Chemistry (with InfoTrac Printed Access Card)
Organic Chemistry : Student Guide and Study Manual
Organic Chemistry and CW+ GradeTracker Access Card Package (6th Edition)
Solutions Manual Organic Chemistry
Organic Chemistry

ASIN: 049501334X

Book Description

This proven and well-tested laboratory manual for organic chemistry students contains procedures for both miniscale (also known as small scale) and microscale users. This lab manual gives students all the necessary background to enter the laboratory with the knowledge to perform the experiments with confidence. For the microscale labs, experiments were chosen to provide tangible quantities of material, which can then be analyzed. Chapters 1-2 introduce students to the equipment, record keeping, and safety of the laboratory. Chapters 3-6, and 8 are designed to introduce students to laboratory techniques needed to perform all experiments. In Chapters 7 and 9 through 20, students are required to use the techniques to synthesize compounds and analyze their properties. In Chapter 21, students are introduced to multi-step syntheses of organic compounds, a practice well known in chemical industry. In Chapter 23, students are asked to solve structures of unknown compounds. The new chapter 24 introduces a meaningful experiment into the textbook that reflects the increasing emphasis on bioorganic chemistry in the sophomore-level organic lecture course. This experiment not only gives students the opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide but also provides valuable experience regarding the role of protecting groups in effecting synthetic transformations with multiple functionalized molecules.

Customer Reviews:

A great help.......2000-06-26

This book writen by Gilbert and Martin provides an excellent help to the student who is currently studying organic chemistry. It is full of useful information and it provides assistance for the completion of the organic labs. it is full of helpful pointers and they provide alot of useful knowledge

Experimental Design for Combinatorial and High Throughput Materials Development

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Experimental Design for Combinatorial and High Throughput Materials Development

Manufacturer: Wiley-Interscience
ProductGroup: Book
Binding: Hardcover

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ASIN: 0471203432

Book Description

In the past decade, combinatorial and high throughput experimental methods have revolutionized the pharmaceutical industry, allowing researchers to conduct more experiments in a week than was previously possible in a year. Now high throughput experimentation is rapidly spreading from its origins in the pharmaceutical world to larger industrial research establishments such as GE and DuPont, and even to smaller companies and universities. Consequently, researchers need to know the kinds of problems, desired outcomes, and appropriate patterns for these new strategies. Editor James Cawse’s far-reaching study identifies and applies, with specific examples, these important new principles and techniques.

Experimental Design for Combinatorial and High Throughput Materials Development progresses from methods that are now standard, such as gradient arrays, to mathematical developments that are breaking new ground. The former will be particularly useful to researchers entering the field, while the latter should inspire and challenge advanced practitioners. The book’s contents are contributed by leading researchers in their respective fields. Chapters include:

-High Throughput Synthetic Approaches for the Investigation of Inorganic Phase Space
-Combinatorial Mapping of Polymer Blends Phase Behavior
-Split-Plot Designs
-Artificial Neural Networks in Catalyst Development
-The Monte Carlo Approach to Library Design and Redesign

Book Description

In this reference leaders at the forefront of research provide an insight into one of the hottest topics in organic synthesis, focusing on the most important enantioselective reactions.
Clearly structured, each entry begins with a concise introduction, including a mechanistic discussion of the reaction, followed by preparative guidelines for newcomers, such as carefully selected working procedures with critical notes for bench chemists, rules of thumb and tips and tricks.

Techniques and Experiments for Organic Chemistry

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Great Text
Great Help
Organic chemistry

Techniques and Experiments for Organic Chemistry
Addison Ault
Manufacturer: University Science Books
ProductGroup: Book
Binding: Hardcover

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Organic Chemistry, Student Study Guide and Solutions Manual
Organic Chemistry
The Organic Chem Lab Survival Manual, A Student's Guide to Techniques
Advanced Practical Organic Chemistry
Organic Chemistry: Structure and Reactivity

ASIN: 0935702768

Book Description

Like its previous five editions, this book is ideally suited for use in a sophomore-level laboratory course in organic chemistry.

Customer Reviews:

Great Text.......2003-12-13

An excellent book for organic chemsitry students. This is the definitive lab manual for beginning o-chem students. A must have for any chemistry undergrad!

Great Help.......2003-12-13

This manual is a wonderful tool for any undergraduate chemistry major going through their beginning organic chemsitry courses.

Organic chemistry.......2001-07-11

When I saw the title of this book I wanted to look at its contents. So, it is excelent. Congratulations!

Lignin: Properties and Materials (Acs Symposium Series)

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Lignin: Properties and Materials (Acs Symposium Series)

Manufacturer: An American Chemical Society Publication
ProductGroup: Book
Binding: Hardcover

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ASIN: 0841216312

Book Description

This volume brings together the current research on all aspects of lignins, the second most abundant group of biopolymers. It covers recent progress in elucidating some of the more intractable aspects of lignin preparation. Among the topics covered in its 41 chapters are: various methods for
studying the structure of lignins; discussions of polymer products derived from the modification of lignin; water-soluble polymers; organosolv pulping, wood adhesives, and enzymatic lignin modification; and various products from lignins, including polyols, polyurethanes, polyblends, grafts, epoxies,
and acrylics.

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