Book Description
Originally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book:
- Uses a problem-solving approach with extensive reference charts and tables.
- Offers an extensive set of real-data problems offers a challenge to the practicing chemist
Customer Reviews:
Excellent excercises..........2006-03-12
It's an OK book if you are a novice in the Spectroscopy determination area, but a very nice book if it's going to be used as a reference book. It's very handy and explains the principles of the Spectroscopic and Spectrometric determinations in a very understandable way. Moreover, the excercises are challenging, making this book and excellent tool for those students interested in learning how to determine structures out of some spectra, although the spectra sometimes are so clean that they don't correspond with the one's that are taken by routine. The weak points of this book are the IR chapter and the lack of a UV chapter explaining various useful techniques for structural determination such as ORD and CD. The NMR section is just OK, but there are more details to be explained in the 2-D NMR NOESY, TOCSY and ROESY. I think the Mass Chapters are the best that any single book has offered to me so far to understand quite easily how powerful is the GCMS as a tool for the Structural Determination of Organic Compounds.
Reference vs. Teaching Material.......2005-03-05
This book has wonderful charts and tables for quick referencing, however it is sorely lacking in demonstrations and worked out examples for students new to the subject. The chapters are painfully slow and complex when explaining the theory behind the spectrometric methods and effects on classes of molecules. In short, don't use this book to learn the material unless you already know it. It is a comprehensive reference, but not an effective textbook to teach from.
Great material, regular text..........2001-07-17
The book is subdivided into only 3 of the 4 classical methods for spectrometric identification of compounds: IR, MS, and finally NMR (covering 1H, 13C and very little of 19F and 31P). UV is left out in this edition, so maybe getting a hold of the old edition's UV chapter (which is extremely well-written) might be desired. The MS and the IR chapters are also well-written and explained out. It is in the main technique (NMR) that the author fails to deliver the subject in a straightforward manner and lacks what I think is most important in this field: a large number of exercises and problems.
An Important book.......2000-05-10
This book provide a the basis of the fundamentals of Spectroscopy in many fields (IR, HNMR, CNMR, DEPT, COSY, HMBC, HMQC, TOCSY, MS, and much more) It has many real problems in an special chapter. And the most important, it has a lot of important tables and spectrums.
Good in NMR Spectra analysis information, but weak elsewhere.......1999-11-19
This book lacked information in my opinion. Silverstein started a good project but just didn't give enough information about IR interpretation, mass spec, C-13 NMR, etc. He focussed on 2-D NMR a great deal, and I believe that there are much better textbooks on this subject.
Book Description
The third edition of the established classic text reference, Principles of Fluorescence Spectroscopy, will enhance upon the earlier editions' successes. Organized as a textbook for the learning student or the researcher needing to acquire the core competencies, Principles of Fluorescence Spectroscopy, 3e will maintain the emphasis on basics, while updating the examples to include recent results from the literature. The third edition also includes new chapters on single molecule detection, fluorescence correlation spectroscopy, novel probes and radiative decay engineering.
This full-color textbook features the following:
- Problem sets following every chapter
- Glossaries of commonly used acronyms and mathematical symbols
- Appendices containing a list of recommended books which expand on various specialized topics
- Sections describing advanced topics will indicate as such, to allow these sections to be skipped in an introductory course, allowing the text to be used for classes of different levels
Principles of Fluorescence Spectroscopy, 3 rd edition, is an essential volume for students, researchers, and industry professionals in biophysics, biochemistry, biotechnology, bioengineering, biology and medicine.
Customer Reviews:
Excellent.......2007-05-22
Stellar text. Very thorough and easy to read. New version is in color, and has several new chapters. I'm very happy with the new edition
The Luminescence Bible.......2007-03-09
What's more to say? This is the authoritative, the definitive volume for luminescence experiments from theory to all of the most useful applications. It is readable, dense, useful and indispensable if you do fluorescence, lifetime measurements, energy transfer studies, etc., etc.
A most worthy successor to the first edition.......1999-09-14
In the sixteen years since the appearance of the first edition of Lakowicz's Principles of Fluorescence Spectroscopy, the use of fluorescence as an analytical tool has grown remarkably, especially in instrumentation, available fluorophores, and practical applications. Therefore, it shouldn't be surprising that the second edition of the work has more than doubled in size.
The approach is the same as that in the first edition: fluorescence spectroscopy from the viewpoint of a biophysical chemist. Explanations are clear. References are profuse; they now number well over a thousand and include an additional appendix that cites many books and review articles for additional reading. Figures are also plentiful; no fancy color diagrams a la contemporary biochemistry texts, but basic line drawings, primarily adapted from journal articles.
The first three chapters ("Introduction to Fluorescence", "Instrumentation for Fluorescence Spectroscopy", and "Fluorophores") are an excellent brief (93-page) introduction to the whole field. Most of the remaining 19 chapters are organized around the kinds of photophysical processes and spectroscopic quantities that are relevant to fluorescence. These include very thorough treatments of fluorescence lifetimes, quenching, anisotropy, and energy transfer. There are many examples drawn from journal articles. In addition, the work now covers more of the technological applications of fluorescence, especially in chapters on "Fluorescence Sensing" and "DNA Technology". These give a sense of the great contributions that fluorescence has made to biotechnology.
My own work involves varied applications of fluorescence to biotechnology, and the second edition of Lakowicz is my reference book of choice. It would also be an excellent text for a graduate course on fluorescence in a chemistry or biochemistry department. All in all, this is a most worth successor to the first edition.
Great book, new edition out soon.......1999-06-10
Joe Lakowicz has just finished a thorough revision of this classic work, which should be coming out soon. Highly recommended.
An excellent book for an overview on fluorometry.......1999-05-12
Introduces the reader to the basic physics and physical chemistry of fluorescence phenomena, fluorometry techniques and covers advanced topics as well. An excellent textbook.
Average customer rating:
- Very Informative
- It is bible for understand NMR
- Good NMR text
- A must have for any aspiring NMR jockeys
- Clear first introduction to NMR
|
Spin Dynamics: Basics of Nuclear Magnetic Resonance
Malcolm H. Levitt
Manufacturer: Wiley
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Understanding NMR Spectroscopy
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Nuclear Magnetic Resonance (Oxford Chemistry Primers, 32)
ASIN: 0471489220 |
Book Description
NMR spectroscopy is one of the most important and widely used techniques for the identification of compounds. Based on an established course this core text offers a truly modern and updated approach.
- Provides a comprehensive introduction to the subject
- Includes a multi-disciplinary approach, concentrating on basic principles and concepts
- Contains chapters of worked examples and problems to encourage a fuller understanding of topics
- Offers a pedagogical approach, starting with quarks and nucleons, and moving on to cover NMR imaging, COSY (Correlated Spectroscopy) and NOESY (Nuclear Overhauser Effect Spectroscopy).
As a core subject in many science disciplines, this text will appeal to a wide range of students, as well as practising scientists and technicians. Assuming only a basic knowledge of complex numbers and matrices, it carefully and lucidly aids readers to fully understand this challenging subject.
Customer Reviews:
Very Informative.......2007-01-04
Coming from a purely Physics background, this book is great at explaining in simple English without sounding like it is talking to a complete idiot. I don't appreciate books that are condescending, and this one is not. Very good, well written, and highly recommended!
It is bible for understand NMR.......2006-11-10
It is a distinguished book for beginer to under stand NMR from theory to experiment step by step.
Good NMR text.......2004-10-05
This is an excellent text book written by a chemist. Author handles some of hardware stuff as well as physical chemistry of NMR based on quantum mechanics. This text provides us with clear pictures of NMR phenomena. Some detailed explanations about basic NMR pulse sequences are excellent for everybody who studies this field.
A must have for any aspiring NMR jockeys.......2004-01-18
For those studying biomolecules with NMR, the unofficial bible is of course the maroon colored Cavanagh book. Though this is an excellent book, it isn't the best suited book for beginners. This is where Levitt's book comes in: this is by far the kindest introduction to NMR that I have seen, with heavy emphasis on understanding the concepts first and the formalism later. The book is full of useful diagrams, detailed analogies, and exercises for the reader where other books only show equations. So borrows someone's Cavanagh first, and if you get stuck after 20 pages then order yourself a copy of Levitt and you won't be disappointed. If you already have studied NMR and are looking at how to apply it to proteins, then Cavanagh should suit you fine.
Clear first introduction to NMR.......2002-07-27
This book could simply be stated as an excellent attempt to introduce the foundations of NMR. It is a very good primer on all theoretical aspects that are essential to an understanding of the subject.
It offers a methodical, step-by-step approach. Useful tools and consistent terminology are the most attracting feature of this volume. It is well-illustrated; and controversial issues are highlighted in the "Notes" sections at the end of each chapter. It has illustrative problems at the end of each chapter, with solutions provided at the end.
Interestingly, the appendix covers many important aspects that are needed at a more advanced stage. Useful tools for the understanding of NMR are developed at appropriate stages. These include: the box notation for coherences, populations, density matrices and transitions; the origin of NMR spectra from individual coherence terms in the density matrix; origin of 2-D NMR signals as well as many important concepts in Fourier Transform NMR are described. The origins of relaxation enjoy a very readable and simplistic approach in the last chapter.
Whenever simplistic approximations are used, the author never claims of completeness or rigour. Distinction is made between terms that are physically correct and terms that are sometimes misleading, but enjoy widespread use in the NMR spectroscopy convention. The essential tools in quantum mechanics are outlined, product operator descriptions are used frequently and repetitively, that enhances understanding and provides more practice. Pictorial representations have been given where possible, a view-point beginners like myself find very useful.
One drawback, is a careful side-lining of the very important technique of using pulse-field gradients, although their cousin technique, named pulse-cycles is quite elaborately explained. I hope, the next issue of the book would also cover up this important technique.
Average customer rating:
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The Raman Effect: A Unified Treatment of the Theory of Raman Scattering by Molecules
Derek A. Long
Manufacturer: Wiley
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Binding: Hardcover
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ASIN: 0471490288 |
Book Description
Presents a unified theoretical treatment, which is complete and rigorous but nonetheless readable. The theoretical treatment requires a variety of mathematical and physical tools. To keep the main text uncluttered, these tools are developed in comprehensive Appendices to which cross-references are made in the main text. These Appendices also ensure that the main text is useful to readers with a wide variety of scientific backgrounds and experience. These include not only spectroscopists, but also chemists, physicists, biochemists and analytical chemists. The presentation is such that postgraduate and postdoctoral students as well as more established research workers will find it valuable.
About the Author
The author was formerly Professor of Structural Chemistry and Director of the Molecular Spectroscopy unit in the University of Bradford. He is distinguished for his original scientific work in a number of areas of Raman spectroscopy. His book, 'Raman Spectroscopy', published in 1978 and long out of print, was highly successful. He has been co-editor of many books including the Specialist Reports on Molecular Spectroscopy, published by the Royal Society of Chemistry; he retired as Editor-in-Chief of the Journal of Raman Spectroscopy in December 1999.
Average customer rating:
- Organic Spectroscopy Made Clear
|
Organic Structure Analysis (Topics in Organic Chemistry)
Phillip Crews ,
Jaime Rodriguez , and
Marcel Jaspars
Manufacturer: Oxford University Press, USA
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ASIN: 0195101022 |
Book Description
Organic Structure Analysis is an ideal text for upper-level undergraduate and first-year graduate courses in organic spectroscopy. It provides students with the background necessary to effectively apply spectroscopic data in establishing features of molecular structure. Unique in its coverage, it is the only text that emphasizes strategies, interpretation, modern techniques, and problem solving. The text's major aim is to show how spectra can be efficiently examined in order to identify a molecule's major structural elements. It focuses on four techniques which are used on a day-to-day basis by most organic chemists: nuclear magnetic resonance (NMR), mass spectroscopy (MS), infrared (IR), and ultraviolet-visible (UV-VIS). Each chapter provides different perspectives on using spectroscopic data in a step-by-step process to establish structural features such as an overall carbon framework; the presence and location of functional groups; the regiochemistry and stereochemistry of substituents; and, finally, the absolute stereochemistry of chiral centers. Recent advances in NMR and MS have changed the way these components are introduced and used in organic spectroscopy courses. Unlike similar texts, this book provides ample, up-to-date coverage of the latest developments in NMR and MS techniques. Organic Structure Analysis adopts a practical approach to the subject which emphasizes building experience; the authors recognize that a combination of problem solving, access to data from models, and understanding the rules of spectral interpretation helps students to build expertise in structure determination from spectra. It outlines elements of theory, but with an emphasis on those directly relevant to spectral interpretation. The text is divided into three major sections; the first section provides extensive coverage of each of the individual methods, the second section illustrates how the strategies of organic structure are actually applied in ten problems whose solutions are provided, and the third section consists of fifty unsolved problems which range from simple monofunctional compounds to complex natural products.
Customer Reviews:
Organic Spectroscopy Made Clear.......2001-08-24
Crews is not a hardcore treatise of the subject. It does not cover the quantum mechanics behind spectroscopy and the complicated mathematical underneath the concept. Instead it discusses the fundamentals and results of such quantum calculations which apply to identification of organic compounds. Basic concepts of nuclear magnetic resonance, infrared spectroscopy, ultra violet spectroscopy are thoroughly covered with examples and charts. Crews is a splendidly-written, straight-forward work that would be suitable for advanced undergraduates who had finished at least one year of organic chemistry, for those who pursue chemical research, and entering grad students.
Book Description
A true introductory text for learning the spectroscopic techniques of Nuclear Magnetic Resonance, Infrared, Ultraviolet and Mass Spectrometry. It can be used in a stand alone spectroscopy course or as a supplement to the sophomore-level organic chemistry course.
Customer Reviews:
A must-have for learning Spectroscopy!.......2007-08-17
I absolutely LOVE this book. I first bought it for my Junior year analytical chemistry class, and I still use it today in grad school. It is VERY good at explaining NMR theory. Anything I ever needed related to NMR or IR I found in this book. It is by far the most useful chemistry book I own.
Dated.......2003-04-11
Standard textbook outlining most spectroscopic techniques as taught at undergraduate level. However, contains an embarrassingly dated treatment of mass spectrometry which can not have been rewritten since the 1970s. No mention of the biggest MS techniques in use today (electrospray and MALDI), a glaring oversight especially in light of Fenn & Tanaka winning Nobel Prizes in 2002 for just these developments. And time-of-flight instruments having a mass range of 5000 and resolution of 200? Several years before this book was published, commercial machines were available with mass ranges well over 100,000 Da and resolutions of 10,000+. Not only poor, but misleading. Overall, a rather derivative book that seems to have been written largely by consultation of more authoritative work (probably an early edition of Williams & Fleming).
Another Good Reference on Organic Spectroscopy.......2001-08-24
The new edition of Pavis might be the twin to Crews' Organic Structural Analysis. This text discusses the fundamentals of 1H NMR, carbon-13 NMR, infrared spectroscopy, UV spectroscopy. The book also includes a section on 2D NMR. Pavia should not be missed by advanced undergraduate students who pursue research and practicing chemists who need quick reference on interpreting spectra.
An Essential Introductory Reference.......2001-05-22
This book is probably the best introductory reference on spectroscopy currently available, and I've checked out pretty much every book on the market right now. I'm a chemist, and this book got me through my senior synthesis and spectroscopy lab. Proton and carbon-13 NMR, IR, GC/MS, and UV/Vis are all covered in the book. It includes many handy tables of characteristic shifts for NMR, characteristic absorbances for IR and UV/Vis, and a nifty table on common GC/MS fragments by m/e. The chapter on 2D NMR is lousy, but that's not really introductory material anyhow. The UV/Vis chapter is kind of cursory, but UV/Vis isn't all that useful.
This is a book that I intend to hang on to for a while.
Great books for students in chemistry.......1999-06-05
I have found this book to a great tool for students of organic chemistry especially those wanting to further their education in graduate school or medical school.It is eay to read and can also be used a "teach yourself" book. I recomend this book to anyone who is a bit shaky in interpreting NMR, IR, and Mass Spec.
Book Description
A skillful balance of theoretical considerations and practical know-how
Backed by a team of expert contributors, the Second Edition of this highly acclaimed publication brings a solid understanding of impedance spectroscopy to students, researchers, and engineers in physical chemistry, electrochemistry, and physics. Starting with general principles, the book moves on to explain in detail practical applications for the characterization of materials in electrochemistry, semiconductors, solid electrolytes, corrosion, solid-state devices, and electrochemical power sources. The book covers all of the topics needed to help readers identify whether impedance spectroscopy may be an appropriate method for their particular research problem.
The book helps readers quickly grasp how to apply their new knowledge of impedance spectroscopy methods to their own research problems through the use of unique features such as:
* Step-by-step instructions for setting up experiments and then analyzing the results
* Theoretical considerations for dealing with modeling, equivalent circuits, and equations in the complex domain
* Best measurement methods for particular systems and alerts to potential sources of errors
* Equations for the most widely used impedance models
* Figures depicting impedance spectra of typical materials and devices
* Extensive references to the scientific literature for more information on particular topics and current research
This Second Edition incorporates the results of the last two decades of research on the theories and applications of impedance spectroscopy. Most notably, it includes new chapters on batteries, supercapacitors, fuel cells, and photochromic materials. A new chapter on commercially available measurement systems reflects the emergence of impedance spectroscopy as a mainstream research tool.
With its balanced focus on both theory and practical problem solving, Impedance Spectroscopy: Theory, Experiment, and Applications, Second Edition serves as an excellent graduate-level textbook as well as a hands-on guide and reference for researchers and engineers.
Download Description
A skillful balance of theoretical considerations and practical know-how Backed by a team of expert contributors, the Second Edition of this highly acclaimed publication brings a solid understanding of impedance spectroscopy to students, researchers, and engineers in physical chemistry, electrochemistry, and physics. Starting with general principles, the book moves on to explain in detail practical applications for the characterization of materials in electrochemistry, semiconductors, solid electrolytes, corrosion, solid-state devices, and electrochemical power sources. The book covers all of the topics needed to help readers identify whether impedance spectroscopy may be an appropriate method for their particular research problem. The book helps readers quickly grasp how to apply their new knowledge of impedance spectroscopy methods to their own research problems through the use of unique features such as: * Step-by-step instructions for setting up experiments and then analyzing the results * Theoretical considerations for dealing with modeling, equivalent circuits, and equations in the complex domain * Best measurement methods for particular systems and alerts to potential sources of errors * Equations for the most widely used impedance models * Figures depicting impedance spectra of typical materials and devices * Extensive references to the scientific literature for more information on particular topics and current research This Second Edition incorporates the results of the last two decades of research on the theories and applications of impedance spectroscopy. Most notably, it includes new chapters on batteries, supercapacitors, fuel cells, and photochromic materials. A new chapter on commercially available measurement systems reflects the emergence of impedance spectroscopy as a mainstream research tool.
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Spectroscopic Methods in Bioinorganic Chemistry (Acs Symposium Series)
Manufacturer: An American Chemical Society Publication
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ASIN: 0841235600 |
Book Description
This volume contains recent advances in spectrographic methods, including EPR, magnetic Mossbauer, paramagnetic and multi-D NMR, metalloprotein crystallography, EAS, magnetic circular dichroism, resonance Raman, X-ray absorption spectroscopy, and electron structure calculations. The book concentrates on topics where spectrographic methods have had a major impact, such as electron transfer, cluster interactions, intermediates, and definition of active site structure, and it includes a thorough tutorial on basic methods.
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Handbook of Phosphorus-31 Nuclear Magnetic Resonance Data
Manufacturer: CRC Press
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ASIN: 0849335310 |
Book Description
To fully utilize Nuclear Magnetic Resonance (NMR) spectroscopy, a comprehensive and well-organized compilation of NMR data is necessary. While compilations have been available for other important NMR nuclei, such as carbon and fluorine, no comprehensive collection of data has been prepared for phosphorus-until now. The CRC Handbook of Phosphorus-31 Nuclear Magnetic Resonance Data provides a collection of 31P NMR chemical shifts for nearly 20,000 organic and inorganic phosphorus compounds. Each class of phosphorus compound is discussed. Bond types, stereochemistry (with the exception of metal complexes), media, important coupling constants, and data sources are included. The information is systematically organized according to coordination state, the atoms bound to phosphorus, and their connectivities. A comprehensive series of bar charts is also included to allow structure types to be assigned to chemical shift data. This handbook is an invaluable resource for all scientists working with phosphorus compounds, including chemists, biochemists, medical researchers, and pharmaceutical chemists.
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Proton and Carbon NMR Spectra of Polymers
Quang Tho Pham ,
Roger Pétiaud ,
Hugues Waton , and
Marie-France Llauro-Darricades
Manufacturer: Wiley
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ASIN: 0470850752 |
Book Description
Represents the largest collection of polymer NMR spectra available
This unique source of information provides a fingerprint of individual polymers, so the microstructure or fine structure of the polymer can be readily identified. Appropriate NMR analysis conditions (solvent(s), temperature, pulse angle, etc.) are specified for each polymer sample. All the resonances, often obtained at different frequencies, are interpreted with remarks concerning the homopolymer or copolymer skeletons.
- Contains over 530 1H and 13C NMR spectra of soluble and swollen gelled 13C polymers
- Includes new NMR polymer spectra, together with those previously published
- Comprehensive bibliography
- Spectra are grouped into families for ready-searching
- CD-ROM is fully searchable and user-friendly
- 5th Edition of popular reference work
An essential reference for polymer chemists and physicists in research and industrial analytical laboratories.
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